All posts by Captain Corrosion

Hot Filament Ionization Gauge

 

The hot-filament ionization gauge is widely used for measuring the level of vacuum. The electrons are emitted from a hot cathode and accelerated towards the anode. In that process the electron may ionize a gas molecule. That gas molecule is pulled towards the collector and ion current is measured with an ammeter.

Penning Ionization Gauge

 

The Penning Ionization Gauge, also known as cold cathode gauge is used to measure the level of vacuum. High voltage between the anode and the cathode causes gas discharge and the resulting ionic current is measured with an ammeter. The measured amperes are then converted into pressure units such as Pascals or Torrs.

Thermocouple Gauge

 

The thermocouple gauge is a device used to measure low vacuum. A filament is heated up by passing a current through it. When gas molecules interact with the filament, heat is carried away. Therefore higher pressure in the chamber means that more heat is taken away. The temperature of the filament can be measured with a thermocouple where the generated voltage depends on the temperature. Therefore in this system the voltage of the thermocouple is measured and converted into pressure units like millibars or pascals.

Pirani Gauge

 

The Pirani Gauge is used to measure low vacuum. In the system tungsten filaments are heated up by passing current through them. As gas molecules interact with the filament, heat is carried away and electrical resistance changes. Therefore if the measured current or voltage can be converted into pressure units.

Diaphragm Pump

 

Diaphragm pump (membrane pump) is an oil-free vacuum pump that is used for obtaining ‪#‎prevacuum‬ of about 0.5 mbar. The pumping in this device is based on the movement of the membrane. As the membrane is pulled down, the volume of the chamber increases, causing a drop of pressure and gas enters the chamber through the inlet. Next, the inlet is closed, outlet opened and the membrane pushed up. This causes the volume of the chamber to decrease and pressure to increase. So the gas is forced to leave the system through the outlet.

Sorption Pump

 

The sorption pump is an oil-free ‪#‎prevacuum‬ pump that is based on the adsorption of gases on cold surfaces. The colder the surface, the more efficient the pumping is! Therefore liquid nitrogen with a temperature less than 77 degrees Kelvin is used for cooling the adsorber. The adsorber is a porous zeolite with a very large surface area as the pores have a diameter in the range of a few nanometers (or less). If the pump is full, then it needs to be renewed by degassing, which is basically heating the adsorber so that the gas can remove the pump through the outlet.

Rotary Vane Pump

 

Rotary Vane Pump is an oil-based vacuum pump, that can be used to obtain ‪#‎prevacuum‬ or even medium vacuum (depending on the system). In this device the rotor and vane(s) are in the housing, that is filled with oil. When the gas enters the chamber through the inlet, it gets trapped in the oil and is transported through the working chamber with the help of the rotor and vane(s) to the outlet, where the gas exits the system. The oil acts as a lubricant and also allows the pumping of some corrosive gases, as it protects the metal to some degree. Although this pump is quite fast and efficient for obtaining pre vacuum, it also may contaminate the vacuum system with oil. Therefore the use of oil traps is highly recommended.

Scroll Pump

 

Scroll pump (scroll compressor) is an oil-free vacuum pump used for obtaining ‪#‎prevacuum‬ with a level of 0.1 mbar. The ‪#‎scrollpump‬ is based on two scrolls, that are placed insede the working chamber. One of these scrolls is fixed and the other one mobile. Once the gas enters the system through the inlet, it gets carried to the outlet in the middle by the mobile orbiting scroll. This is possible due to the fact that during the mobile scrolls movement a wide gap is locally kept between the two scrolls and the gap moves to the middle, carrying the gas in it. As the volume of the gap decreases at the outlet, the gas is pushed out of the system. Due to wear the orbiting scroll needs to be replaced about twice a year.

Cryopump

 

The ‪#‎cryopump‬ is a high vacuum pump that is based on the adsorption of gas on cold surfaces. The cooler the surface – the better the pumping! For that purpose liquid helium is often used for cooling the system parts as it is extremely cold, having a temperature only four degrees above absolute zero. The pumping is done in multiple stages, where each stage has a different temperature. The „warmest“ part is the first stage, that has a temperature of 100 degrees Kelvin (or lower) and that causes water to condensate on it. During the ‪#‎condensation‬ of water also some other gases may also be trapped under the water and that process is called ‪#‎cryotrapping‬. However, in order to effectively pump gases such as nitrogen, even colder surfaces (less than 17 degrees Kelvin) are required. In this stage the metal may also be coated with porous activated charcoal and that allows to adsorb even smaller gas molecules such as helium and even hydrogen (this is called ‪#‎cryosorption‬ ). So basically the pumping of gases with this ‪#‎vacuumpump‬ is based on three processes: condensation, cryotrapping and cryosorption.

Titanium Sublimation Pump

The titanium sublimation pump is a vacuum pump used as a part of vacuum systems in order to briefly improve the level of ‪#‎vacuum‬. The working principle is relatively simple. A pulsing current passes through a titanium filament, causing it to sublimate (goes directly from solid phase to gas phase). The fresh titanium chemically reacts with gas in the vacuum chamber, creating a solid product that deposits on the chamber walls. As the walls are also coated with highly reactive freshly deposited titanium, they may also chemically bind gas molecules that interact with them. Some gases may not chemically bind with titanium but can still be physically trapped under the titanium atoms on the chambers walls.